CHL 201- Laboratory for Organic Chemistry I

Fall Semester, 2003

 

Section 41:  Thomas S. Straub, Ph.D.

Sections 42, 43, 44:  William A. Price, Ph.D.

 

Date                           Experiment

 

Aug 25-27                  Check-in Safety.

 

Sept 2-3,8                  EXP 1, Extraction of Caffeine from Tea, pp 3-6.

 

Sept 9-10,15             EXP 4, Synthesis of Salicylic Acid, pp 19-23.

 

Sept 16-17,22           EXP 5, Synthesis of Aspirin, pp 27-30.

 

Sept 23-24,29           PROJECT 3.1, Hydrolysis of an Unknown Ester: Hydrolysis and Azeotropic Distillation, pp 247-252.

 

Sept 30, Oct 1,6        PROJECT 3.2, Extraction and Recrystallization, pp 252-254.

 

Oct 7-8,13                  PROJECT 3.3, Distillation, Boiling Points, Melting Points, and Identification, pp 254-258.

 

Oct 14-15,27             EXP 16.1, Free-Radical versus Ionic Addition of HBr to Alkenes, pp 133-139.

 

Oct 20-22                   Mid-Semester Break.

 

Oct 28-29, Nov 3       EXP 6.2, Isolation of  (R)-(+)-Limonene from Orange Peels, pp 37-39, 44-46.

 

Nov 4-5,10                 EXP 8.1, Radical Chlorination Reactions, pp 57-63.

 

Nov 11-12,17             EXP 11.2, Acid-Catalyzed Dehydration of 3-Methylcyclohexanol, pp 83-86, 89-91.

 

Nov 18-19,24             EXP 9.1, SN1/SN2 Reactivity of Alkyl Halides, pp 67-71.

 

Nov 25-26                  Thanksgiving Holiday!

 

Dec 1-3                      Check-out.  All laboratory reports due.