CHL 201- Laboratory for Organic Chemistry I
Fall Semester, 2009
Sections 41, 42: William A. Price,
Ph.D.
Section 43, 44: Thomas S. Straub, Ph.D.
Mohrig, Hammond, Schatz and
Morrill, Modern Projects in Organic Chemistry, 2nd edition, W.H.
Freeman, New York, 2003.
DATE |
EXPERIMENT |
Sept. 1-3 |
Safety, Check-in |
Sept. 8-10 |
EXP 1, Extraction of Caffeine from Tea, pp 3-6. |
Sept. 15-17 |
Handout, Separation of the Components of a Trinary Mixture.
Acid/Base Chemistry |
Sept. 22-24 |
EXP 5, Synthesis of Aspirin, pp 27-30. |
Sept. 29-Oct.1 |
PROJECT 3.1, Hydrolysis of an Unknown Ester:
Hydrolysis and Azeotropic Distillation, pp 247-252. |
Oct. 6-8 |
PROJECT 3.2, Extraction and Recrystallization,
pp 252-254. |
Oct. 13-15 |
PROJECT 3.3, Distillation, Boiling Points, Melting
Points, and Identification, pp 254-258. |
Oct 21-22, 27 |
EXP 16.1, Free-Radical versus Ionic Addition of HBr to Alkenes, pp 133-139. |
Oct 28-29, Nov. 3 |
EXP 6.2, Isolation of (R)-(+)-Limonene from Orange Peels,
pp 37-39, 44-46. |
Nov 4-5, 10 |
EXP 6.2,
continued. |
Nov 11-12, 17 |
EXP 8.1, Radical Chlorination Reactions, pp 57-63. |
Nov 18-19, 24 |
EXP 11.2, Acid-Catalyzed Dehydration of
3-Methylcyclohexanol, pp 83-86, 89-91. |
Dec. 1-3 |
EXP 9.1, SN1/SN2 Reactivity of Alkyl Halides, pp
67-71. |
Dec. 8-10 |
Check-out. All laboratory reports due. |