CHL 201- Laboratory for Organic Chemistry I
Fall Semester, 2009

Sections 41, 42: William A. Price, Ph.D.
Section 43, 44: Thomas S. Straub, Ph.D.

Mohrig, Hammond, Schatz and Morrill, Modern Projects in Organic Chemistry, 2nd edition, W.H. Freeman, New York, 2003.

DATE

EXPERIMENT

Sept. 1-3

Safety, Check-in

Sept. 8-10

EXP 1, Extraction of Caffeine from Tea, pp 3-6.

Sept. 15-17

Handout, Separation of the Components of a Trinary Mixture.  Acid/Base Chemistry

Sept. 22-24

EXP 5, Synthesis of Aspirin, pp 27-30.

Sept. 29-Oct.1

PROJECT 3.1, Hydrolysis of an Unknown Ester: Hydrolysis and Azeotropic Distillation, pp 247-252.

Oct. 6-8

PROJECT 3.2, Extraction and Recrystallization, pp 252-254.

Oct. 13-15

PROJECT 3.3, Distillation, Boiling Points, Melting Points, and Identification, pp 254-258.

Oct 21-22, 27

EXP 16.1, Free-Radical versus Ionic Addition of HBr to Alkenes, pp 133-139.

Oct 28-29, Nov. 3

EXP 6.2, Isolation of (R)-(+)-Limonene from Orange Peels, pp 37-39, 44-46.

Nov 4-5, 10

EXP 6.2, continued.

Nov 11-12, 17

EXP 8.1, Radical Chlorination Reactions, pp 57-63.

Nov 18-19, 24

EXP 11.2, Acid-Catalyzed Dehydration of 3-Methylcyclohexanol, pp 83-86, 89-91.

Dec. 1-3

EXP 9.1, SN1/SN2 Reactivity of Alkyl Halides, pp 67-71.

Dec. 8-10

Check-out. All laboratory reports due.