CHL 202 – Organic Chemistry II Laboratory

Summer Session II, 2014

Text: La Salle University CHL 201-202 Laboratory Manual (Custom text from Freeman Publishing), adapted from Mohrig, Schatz and Morrill, Modern Projects and Experiments in Organic Chemistry, Freeman, New York, 2003).

Instructors: Laura Grande and William Price

Date Experiment

June 30 Exp. 16: Interconversion of 4-tert -butylcyclohexanol and 4-tert butylcyclohexanone. Part 1: Oxidation

July 2 Exp. 16: continued. Part 2: Reduction

July 3 Exp. 14: Grignard Synthesis of Secondary and Tertiary Alcohols

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July 7 Exp. 14: continued

July 9 Exp 15: Phase Transfer Catalysis: Synthesis of Butyl Benzoate

July 10 Spectroscopy Workshop – Mass, IR, ¹H NMR, ¹³C NMR

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July 14 Exp. 11: Diels-Alder Reaction

July 16 Exp 13: Acylation of Ferrocene

July 17 Exp 13: continued

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July 21 Exp 17: Synthesis of a Mosquito Repellant: N,N-Diethyl-meta-toluamide

July 24 Exp 18: Aldol-Dehydration Chemistry Using Unknown Aldehydes and Ketones

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July 28 Exp 18: continued: Preparation and Characterization of Solid Derivatives