CHL 202
Laboratory for Organic Chemistry II
Spring , 2010
Text: Morhig,
Hammond, Schatz, and Morrill, Modern Projects and Experiments in Organic
Chemistry, Freeman, New York, 2003.
Instructors: Thomas S. Straub, Ph.D., William A. Price,
Ph.D.
Date
|
Experiment
|
|
Jan.
19,20 |
EXP
19 Diels-Alder Reaction |
|
Jan.
26,27 |
EXP
20 Selectivity in the Bromination
of Acetanilide |
|
Feb.
2,3 |
EXP
21 Acylation of Ferrocene |
|
Feb.
9,10 |
EXP
21 continued |
|
Feb.
16,17 |
PROJECT
5.2 Grignard Synthesis of Secondary and
Tertiary Alcohols |
|
Feb.
23,24 |
PROJECT
5.2 continued |
|
March
2,3 |
PROJECT
4 Interconversion of 4-tert-Butylcyclohexanol
and 4-tert-Butylcyclohexanone.
4.1 Green Chemistry: NaOCl Oxidation |
|
March
8-12 |
SPRING
BREAK |
|
March
16,17 |
PROJECT
4 4.2 Sodium Borohydride
Reduction |
|
March
23,24 |
EXP
18 Phase Transfer Catalysis: Synthesis of
Butyl Benzoate |
|
March
30,31 |
Exp
28.2 Synthesis of a Mosquito
Repellant: N,N-Diethyl-meta-toluamide (DEET) |
|
April
6,7 |
EXP
28.2 continued |
|
April
13,14 |
PROJECT
11 Aldol-Dehydration Chemistry
Using Unknown Aldehydes and Ketones. 11.1 Preparation and Characterization of Aldol-Dehydration Condensation Product |
|
April
20,21 |
PROJECT
11 11.2 Preparation and Characterization of
Solid Derivatives of the Unknown Aldehyde and Ketone |
|
April
27,28 |
Check-out. All laboratory reports due! |